您目前所在的位置:首页 - 期刊简介 - 详细页面

铁道科学与工程学报

JOURNAL OF RAILWAY SCIENCE AND ENGINEERING

Vol. 19    Special 1    September 2009

[PDF Download]    [Flash Online]

    

Synthesis and microstructure of zirconia nanopowders by glycothermal processing
Jun-Seop KIM1, Dong-Hae LEE1, Sung KANG1, Dong-Sik BAE1, Hoy-Yul PARK2, Moon-Kyeung NA2

1. School of Nano & Advanced Material Engineering, College of Engineering, Changwon National University,
Gyeongnam 641-773, Korea;
2. Advanced Materials and Application Research Laboratory, Korea Electro Technology Research Institute,
Changwon 641-600, Korea

Abstract:ZrO2 nanoparticles were prepared under high temperature and high pressure conditions by precipitation from metal nitrates with aqueous potassium hydroxide. The effects of synthesis parameters, such as the concentration of starting solution, pH of starting solution, reaction temperature and time, were discussed. The results show that the ZrO2 nanoparticles are obtained at 230−270 ℃. The average size and size distribution of the synthesized particles are below 10 nm and narrow, respectively. The XRD pattern shows that the synthesized particles are composed of crystalline. The synthesis of ZrO2 nanosized crystalline particles is possible under glycothermal conditions in ethylene glycol solution.

 

Key words: ZrO2 nanoparticles; glycothermal processing; particle size; microstructure

ISSN 1672-7029
CN 43-1423/U

主管:中华人民共和国教育部 主办:中南大学 中国铁道学会 承办:中南大学
湘ICP备09001153号 版权所有:《铁道科学与工程学报》编辑部
------------------------------------------------------------------------------------------
地 址:湖南省长沙市韶山南路22号 邮编:410075
电 话:0731-82655133,82656174   传真:0731-82655133   电子邮箱:jrse@mail.csu.edu.cn